Structural characterization of wheat straw lignin as revealed by analytical pyrolysis, 2D-NMR, and reductive cleavage methods.

By J. D. del Río, J. Rencoret, P. Prinsen, Angel T. Martı́nez, J. Ralph, A. Gutiérrez. Journal of Agricultural and Food Chemistry, 2012

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Structural analysis for lignin characteristics in biomass straw (2013, background): “The HSQC approaches have also been valuable in assigning major structures of non-acetylated lignin from different origins in recent years, such as some non-woody plants [32], Jute fibres [82], bamboo [84,85,87], Triploid poplar [88e90] and wheat straw [83].”
Recent Advances in Characterization of Lignin Polymer by Solution-State Nuclear Magnetic Resonance (NMR) Methodology (2013, background): “For example, the detailed assignments of HSQC spectra of non-acetylated (Figure 4) and acetylated bamboo lignin samples of bamboo MWL (Figure 5) are listed in Table 2 and the major substructures are depicted in Figure 6 based on recent studies [41,45,51,52].”
Recent innovations in analytical methods for the qualitative and quantitative assessment of lignin (2015, methodology): “Guaiacol derivative (G-C3H3), 4-allenylguaiacol 162/147 G [59,298,299]”