Decacarbonyl‐μ‐hydrido‐μ‐vinyl‐triangulo‐triosmium: a combined X‐ray and neutron diffraction study

By A. Orpen, D. Pippard, G. Sheldrick, K. Rouse. 1978

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Macromolecular structure determination using X-rays, neutrons and electrons: recent developments in Phenix (2019, methodology): “…called joint X-ray and neutron refinement (joint XN refinement), ameliorates the data-to-parameters ratio by increasing the amount of experimental data used in refinement, leading to more complete and accurate models (Coppens, 1967; Orpen et al., 1978; Wlodawer, 1980; Wlodawer & Hendrickson, 1982).”
Evaluation of models determined by neutron diffraction and proposed improvements to their validation and deposition (2018, background): “…low signal to noise and the increased number of parameters, the concept of joint X-ray and neutron refinement (hereafter referred to as joint XN refinement) was introduced (Coppens, 1967; Orpen et al., 1978; Wlodawer, 1980; Wlodawer & Hendrickson, 1982; Adams et al., 2009; Afonine et al., 2010).”