Characterisation of cement hydrate phases by TEM, NMR and Raman spectroscopy

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Advances in characterizing and understanding the microstructure of cementitious materials (2019, background): “Recent TEM studies have been reported for the cementitious matrix [48–50], lab-synthesized C-(A)S-H [51,52], systems incorporating SCMs such as fly ash [53–56], blast furnace slag [57,58] and silica fume [59].”
Phillipsite and Al-tobermorite mineral cements produced through low-temperature water-rock reactions in Roman marine concrete (2017, methodology): “…of laboratory syntheses of 11 Å tobermorite without aluminum, geologic 11 Å tobermorite from Crestmore, California, and laboratory C-S-H with calcium/silica = 0.8 to 0.83 referenced in previous NMR studies (Kirkpatrick et al. 1997; Richardson et al. 2010; Black 2009; Jackson et al. 2013a, 2013b).”