Metabolomics: back to basics

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NMR-based metabolomic analysis of plants (2010, background): “In freeze-drying, frozen water in the material sublimes under low pressure, and is thus a relatively gentle and mild drying metho”
Ecological metabolomics: overview of current developments and future challenges (2011, methodology): “For more detailed information on the advantages and disadvantages of each method, see Summer et al. (2003), Kopka et al. (2004), Moco et al. (2007) and Verpoorte et al. (2008).”