Cellulose I crystallinity determination using FT–Raman spectroscopy: univariate and multivariate methods

By U. Agarwal, R. Reiner, S. Ralph. 2010

274 citations recorded by the source corpus.

Subfields: Biomaterials, Biomedical Engineering, Plant Science

View Paper: https://www.semanticscholar.org/paper/ee39b160a679b7ff2a24bf29fd10a3abd5c1418c

How researchers see this paper

The researchers whose trusted networks rank it highest, strongest advocate first. Every researcher gets a different order.

In Biomaterials

In Biomedical Engineering

In Plant Science

Citations in the corpus

Cellulose Chemistry and Properties: Fibers, Nanocelluloses and Advanced Materials (2016, background): “In the 1980s, Johnson & Johnson (New Brunswick, USA) started to commercialize sheets of BC on large scale for the treatment of different wounds [42, 43].”
Probing cellulose structures with vibrational spectroscopy (2019, unknown): “17b, c) (Agarwal et al. 2010, 2018).”
Tailoring the yield and characteristics of wood cellulose nanocrystals (CNC) using concentrated acid hydrolysis (2015, methodology): “The samples were also analyzed using Raman spectroscopy to determine CrI (Table S1) based on the ratio of the Raman scattering intensities at 380 and 1096 cm-1 (Agarwal et al. 2010).”
Cellulose polymorphy, crystallite size, and the Segal Crystallinity Index (2013, unknown): “…Southern Regional Research Center, Agricultural Research Service, U.S. Department of Agriculture, 1100 Robert E. Lee Blvd., New Orleans, LA 70124, USA e-mail: al.french@ars.usda.gov Other workers also find fault with the Segal method (Agarwal et al. 2010; Park et al. 2010; Thygesen et al. 2005).”
Mechanical deconstruction of lignocellulose cell walls and their enzymatic saccharification (2013, methodology): “The CNF crystallinity was measured by a FTRaman spectroscopic method (Agarwal et al. 2010) using approximately 0.15 g of air-dried sample pressed into a pellet with a Bruker MultiRam spectrometer (Bruker Instruments Inc., Billerica, MA).”
Effect of sample moisture content on XRD-estimated cellulose crystallinity index and crystallite size (2017, background): “For example, to estimate CrI, NMR (Larsson et al. 1999; Newman 1999; Peciulyte et al. 2015), Raman spectroscopy (Agarwal et al. 2010, 2013, 2014; Schenzel et al. 2005), DSC (Bertran and Dale 1986), sum frequency vibrational spectroscopy (Barnette et al. 2012), terahertz spectroscopy (Vieira and…”