High-efficient Synthesis of Graphene Oxide Based on Improved Hummers Method

By Huitao Yu, Bangwen Zhang, Chaoke Bulin, Ruihong Li, Ruiguang Xing. Scientific Reports, 2016

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As an important precursor and derivate of graphene, graphene oxide (GO) has received wide attention in recent years. However, the synthesis of GO in an economical and efficient way remains a great challenge. Here we reported an improved NaNO3-free Hummers method by partly replacing KMnO4 with K2FeO4 and controlling the amount of concentrated sulfuric acid. As compared to the existing NaNO3-free Hummers methods, this improved routine greatly reduces the reactant consumption while keeps a high yield. The obtained GO was characterized by various techniques, and its derived graphene aerogel was demonstrated as high-performance supercapacitor electrodes. This improved synthesis shows good prospects for scalable production and applications of GO and its derivatives.

Subfields: Biomedical Engineering, Electronic, Optical and Magnetic Materials, Materials Chemistry

View Paper: https://www.semanticscholar.org/paper/cfc0afdc876e239099d7e98ebc7e1265faad8d5a

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In Biomedical Engineering

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