A new approach in quantitative in-situ XRD of cement pastes: Correlation of heat flow curves with early hydration reactions

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Rietveld Quantitative Phase Analysis of OPC Clinkers, Cements and Hydration Products (2012, positive): “This methodology allows understanding the chemical origin of different regions/features in the calorimetric curves (hydration reactions) and also supports the accuracy of RQPA (Hesse et al. 2011).”
Calcined clay – Limestone cements: Hydration processes with high and low-grade kaolinite clays (2021, background): “As described by Hesse et al. [54] on synthetic cement, the total dissolution of anhydrite matches with the second peak observed on heat flow curves occurring during stage III.”
Retardation effect of styrene-acrylate copolymer latexes on cement hydration (2015, methodology): “have intensively contributed to enable a better interpretation of the calorimetric data by following the time-dependent phase evolution during early hydration of cement using the technique of in-situ XRD [21,22].”
Advances in characterizing and understanding the microstructure of cementitious materials (2019, methodology): “…of the phases, in-situ XRD coupled with a Rietveld refinement analysis using an external standard [102] can be preferred and were recently used to better understand the evolution of the chemical balance in the first hours of hydration as well as the effect of admixtures [97,98,100,101,103].”