Introduction of aldehyde groups on surfaces of native cellulose fibers by TEMPO-mediated oxidation

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Mechanical characterization of cellulose nanofiber and bio-based epoxy composite (2012, methodology): “Cellulose nanofibers were prepared according to a procedure described by Saito and Isogai [17].”
Review: Catalytic oxidation of cellulose with nitroxyl radicals under aqueous conditions (2018, methodology): “[133] Hirota M, Tamura N, Saito T, Isogai A. Oxidation of regenerated cellulose with NaClO2 catalyzed by TEMPO and NaClO under acid-neutral conditions.”
Sodium periodate oxidation of cellulose nanocrystal and its application as a paper wet strength additive (2015, background): “Saito and Isogai (2006) investigated the TEMPO oxidation of natural cellulose to generate aldehyde groups on the fiber surfaces and insides of the cellulose fibers, and found that only the surface aldehyde groups contributed to the paper wet strength.”
State of the Art Manufacturing and Engineering of Nanocellulose: A Review of Available Data and Industrial Applications (2013, methodology): “CNs Surface Modification by Oxidation In an attempt to prevent CNs post-aggregation during the spray-drying procedures, several authors reported methods affecting the surface, such as polarity and chemical arrangements therewith, of the cellulose by oxidation processes [32,96-99].”