Strategy for control of crystallization of polymorphs

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Effect of relative humidity on the carbonation rate of portlandite, calcium silicate hydrates and ettringite (2020, background): “At 487 high RH (> 90%) water monolayers form a water film on the particle surface, which allows the 488 calcium carbonate to nucleate in the aqueous layer [23] and may ease recrystallization to the 489 thermodynamically more stable polymorphs aragonite and calcite [69,87,88].”
Synthesis Methods and Favorable Conditions for Spherical Vaterite Precipitation: A Review (2019, background): “The supersaturation can influence the size of the crystallite forming vaterite particles, and a smaller crystal subunit was observed when supersaturation increased [69,70].”