Gram-scale production of graphene based on solvothermal synthesis and sonication.

By Mohammad Choucair, P. Thordarson, J. Stride. Nature Nanotechnology, 2009

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The synthesis of graphene sheets with controlled thickness and order using surfactant-assisted electrochemical processes (2012, methodology): “[24] Choucair M, Thordarson P, Stride JA.”
Experimental Review of Graphene (2011, background): “The individual layer, crystalline, and graphitic nature of the samples was confirmed by TEM, selected area electron diffraction (SAED), and Raman spectroscopy [62].”
Graphene-based materials: synthesis and gas sorption, storage and separation (2015, methodology): “Using the bottom-up solution-phase method, graphenes of gram scales are produced from simple laboratory reagents of sodium and ethanol in a 1:1 M ratio by solvothermal method [259,260].”
Manipulating the electronic and chemical properties of graphene via molecular functionalization (2013, background): “Moreover, the one-step electrochemical exfoliation [29], arc discharge [30], and direct chemical synthesis of graphene have also been realized recently [31].”
Graphene synthesis, characterization and its applications in nanophotonics, nanoelectronics, and nanosensing (2015, background): “Scale bars a 200 nm, b 1,000 nm [60] Fig.”
Graphene nanosheets reduced by a multi-step process as high-performance electrode material for capacitive deionisation (2012, methodology): “[22] Choucair M, Thordarson P, Stride JA.”