Preparation of millimeter-long cellulose I nanofibers with diameters of 30–80 nm from bamboo fibers

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Processing of wood-based microfibrillated cellulose and nanofibrillated cellulose, and applications relating to papermaking: a review (2016, methodology): “High-intensity ultra-sonication (HIUS) Another usefulmechanical technique that has been used to extract cellulose nanomaterials is high-intensity ultrasonication (Mishra et al. 2012; Chen et al. 2011a, b, c; Cheng et al. 2010; Wang and Cheng 2009; Zhao et al. 2007).”
Cellulose nanomaterials: new generation materials for solving global issues (2019, methodology): “Using different output power of the ultrasonication, Chen et al. (2011b) found that high output of 1000 W or above is required to individualize nanofibers (i.e. having widths of 5–20 nm) from chemical purified wood.”
Preparation and characterization of nanocrystalline cellulose via low-intensity ultrasonic-assisted sulfuric acid hydrolysis (2014, methodology): “All of the above results supported the conclusion that the molecular structures of cellulose remained unchanged in the presence of sulfuric acid hydrolysis process and ultrasonic treatment (Chen et al. 2011a).”
Isolation, characterization, and application of nanocellulose from oil palm empty fruit bunch fiber as nanocomposites (2014, background): “[15] as well as those produced by mechanical treatment originating from rutabaga fiber [36], bamboo fiber [44], and rubberwood [31], for which the range of diameter has been reported as 5– 20 nm, 30–80 nm, and 10–90 nm, respectively.”