Preparation of silica nanoparticles: determination of the optimal synthesis conditions for small and uniform particles

By Sung Kyoo Park, Ki Do Kim, H. Kim. 2002

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Nanoparticles: structure, properties, preparation and behaviour in environmental media (2008, background): “It is well known that the base catalysed hydrolysis of tetraethyl orthosilicate results in particles of 10‐350 nm that have a charged surface ( Park et al. 2002 ).”
Synthesis of silica nanoparticles by sol-gel: size-dependent properties, surface modification, and applications in silica-polymer nanocomposites — a review (2012, background): “In principle, smaller nanoparticles are obtained by controlling (slowing down) the rate of polycondensation reactions through manipulation of reaction parameters [19, 24].”
Optimization of parameters for the fabrication of gelatin nanoparticles by the Taguchi robust design method (2008, methodology): “Efficient analyses of this complex system have been performed recently, using statistical experimental design [21] and the Taguchi method [15,17].”