Facile green synthesis of NiO nanoparticles and investigation of dye degradation and cytotoxicity effects

By Zahra Sabouri, A. Akbari, H. Hosseini, M. Darroudi. Journal of Molecular Structure, 2018

183 citations recorded by the source corpus.

Abstract Dispersed nickel oxide nanoparticles (NiO-NPs) have been obtained through a “green” co-precipitation method using nickel nitrate hexahydrate and starch as Ni precursor and stabilizing/capping agent, respectively, while ammonia has been applied in the role of a complex agent throughout this procedure. The structural, photocatalyst, optical, and magnetic qualities of the NiO-NPs have been enquired into by FTIR, UV–Vis, XRD, FESEM, EDX, VSM, and TGA/DTG. Magnetic measurement has confirmed the superparamagnetic behavior of NiO-NPs at ambient temperature after calcination procedures. The band gap of NiO-NPs has been calculated to be about 3.55 eV and thus, this sample is a semiconductor that can be utilized as photocatalysts. According to the obtained results, about 80% of methylene blue (MB) degrades in the presence of NiO-NPs under UV light after 270 min. In vitro cytotoxicity investigations on cells has exhibited a dose-dependent toxicity with non-toxic consequences in concentrations below ∼7 μg/mL. The synthesis outcomes have shown that starch can be an interesting material with the potential of being employed as a stabilizer for preparing small nanoparticles, as well as being a bio-template for nanoparticles growth.

Subfields: Electrical and Electronic Engineering, Materials Chemistry, Polymers and Plastics

View Paper: https://www.semanticscholar.org/paper/1f9cc461874c351a352cfdbaa3ceaf371d8f7cf8

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